法国专利FR3043882A1 PROCESS FOR TREATING SEEDS

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专利摘要:
Seed treatment method, using a composition obtained extemporaneously by mixing at least one pulverulent substance and an aqueous medium, comprising the steps of: - performing automatically and cyclically the mixture in at least a first tank (10; 10 ') by first introducing at least a portion of the aqueous medium and then the powder substance, the latter being sucked into the aqueous medium in the tank through a depression created in the tank, - at least partially emptying, by means of at least one flushing of a compressed gas into the tank, its contents to a seed treatment device where the mixture is brought into contact with the seeds.
公开号:FR3043882A1
申请号:FR1561306
申请日:2015-11-24
公开日:2017-05-26
发明作者:Chenglu David；Patrick Ferlin；Carole Lechartier；Patrick Phelippeau
申请人:Rhodia Operations SAS；
IPC主号:

专利说明:

PROCESS FOR SEEDING TECHNICAL FIELD
The present invention relates to the treatment of seeds and more particularly but not exclusively a method and an installation for preparing a mixture for treating, in particular coating, seeds.
BACKGROUND
In the field of agriculture, it is known to treat seeds to be able to handle them more easily, to improve the environment in which they will develop or their germinative properties, or to protect them, for example vis-à-vis harmful, mold, weather conditions or against deterioration during aging. To do this, different treatment processes exist, such as simple seed dressing, seed coating or seed pelletizing.
The film coating generally consists in depositing on the surface of the seeds a thin film of polymer in which are included various agrochemical substances. The shape and size of the seeds during this process are only slightly modified. Encapsulation generally consists in modifying the size and shape of the seeds by a large input of inert material, for example to facilitate the use of conventional mechanical seeders which have difficulty in being used with seeds that are too small. Several phytosanitary substances can thus be located more precisely in the different layers of the coating.
In the following, we designate by "coating" a "filming" or "capping".
Conventionally, the treatment formulations used are: liquid formulations typically comprising a fungicide dispersed in water, pigments and binding polymers (in English "binders"), or powder formulations, for accelerating the drying, decrease the adhesiveness and improve the fluence of seeds.
Typically, the liquid formulations are applied to the seeds by methods such as spraying, spraying-drying, kneading, churning or any other means well known to those skilled in the art.
In the case of powder formulations, the adhesion of the formulation to the seeds is done by adding water.
Specifically, the most commonly used method is to premix the powder and water to obtain a dispersion, which is then applied to the seeds. Alternatively, you can proceed as follows: either the seeds are wetted and the powder is then added to the seeds, or the powder is mixed with the seeds and then the water is added.
Some treatment compounds, however, remain difficult to apply to seeds. This is the case, in particular, hydratable compounds developing a high viscosity in contact with water and that it is desired to use in a significant mass proportion. Typically, on field seeds, the target proportion is between 0.1% and 1%, this proportion corresponding to the mass of the treatment formulation in dry weight, after removal of water, on the seed mass. .
In the case of a liquid formulation, these hydratable compounds generate a viscosity that is too high to be able to handle and apply the formulation under usual conditions. The option of diluting the formulation (to reduce the concentration of the compound and thus limit the viscosity of the formulation) is, moreover, not satisfactory. Indeed, this option would lead to introduce a significant amount of water compared to the mass of treated seeds. However, the quantity of water is limited by a maximum value acceptable by the seeds in the absence of drying, which is the rule for field seeds. Beyond this acceptable threshold, the seed can germinate spontaneously during storage, quickly losing its germinative capacity after some storage time, or the water can cause the seed to swell, which only returns to its original shape very slowly, these variations volume that can cause crumbling or cracking of the encapsulating film or film coating, or cause agglomerates treated seed. The option of diluting the formulation would therefore be satisfactory only if seeds are used immediately after treatment, which is not an option for field seeds because these seeds represent large volumes.
In the case of a powder formulation, it has been found that the aforementioned hydratable compounds caused problems of inhomogeneity of seed treatment, and residues in turn causing problems of loss of material and fouling of the apparatuses. mixed.
Various facilities for dispersing a powder in a liquid medium have been proposed. EP 1 165 874 discloses an installation in which a powder is introduced into a mixing tank via a dip tube.
Such an installation is however not suitable for the preparation of a composition based on hydratable compound (s), given its rheological behavior. In particular, the use of hydratable compounds would pose a problem of rapid fouling of the dip tube and deposition on the walls of the tank of residues difficult to remove.
The publications CN 202105636, CN 203329707, CN104607091 and CN201880505 describe other facilities also unsuitable for the automatic preparation of several successive batches of mixture, with a relatively low variability of the formulation of the mixture between batches.
There is therefore a need for a new treatment method for the automated and cyclic application of powdery substances, especially hydratable compounds, to seeds in a significant proportion.
There is also a need for an installation for the implementation of such a process on an industrial scale and at a reasonable cost.
There is also a need for an installation which makes it possible to implement, in a combined way, by means of a single installation, different types of seed treatments.
There is also a need for a new seed treatment process, and an installation for the implementation of such a process, which can be integrated into an industrial seed treatment chain without significantly impacting the bulk and / or or the rate (typically at least 20 kg of seed treated per minute, in particular of at least 100 kg of seed treated per minute, in particular of at least 150 kg of seed treated per minute, in particular of at least 200 kg of treated seed per minute or even 300 kg of treated seed per minute).
GENERAL PRESENTATION The invention satisfies all or part of the aforementioned needs by means of a seed treatment process, using a composition obtained extemporaneously by mixing at least one pulverulent substance and an aqueous medium, comprising the steps of: - automatically and cyclically perform the mixture in at least a first tank by first introducing at least a portion of the aqueous medium and then the powder substance, the latter being sucked into the aqueous medium in the tank thanks to a depression created in the tank, - at least partially emptying, by means of at least one flushing of a compressed gas into the tank, its contents to a seed treatment device where the mixture is brought into contact with the seeds. The invention allows automated operation over several cycles of treatment, advantageously limiting the problems of fouling of the vessel related to the rheological behavior of the dispersion in the case where the powder substance is a hydratable compound. The injection of the powder substance into the liquid in the tank through a vacuum is found to limit the emission of dust and the deposition of the powdery substance on the walls of the tank, while ensuring good dispersion of the powdery substance within the liquid. The invention is thus particularly well suited to a pulverulent substance which would be a hydratable compound. The invention is particularly suitable for a mixture which has a viscosity which increases significantly with time.
The volume of the mixture in the tank is preferably less than or equal to 151, more preferably 101, being preferably at least 0.1L, especially at least 0.5L. Such a volume is well suited to seed treatment, and allows the use of a standard manufacturing vessel, without particular strengthening of its mechanical strength, which would not be the case with a larger vessel, given the levels. pressure or depression encountered. It should be noted that surprisingly, despite this relatively small volume, the injection of the powdery substance can be done without fouling the tank or cause a strong dust emission, despite repeated cycles without manual intervention within the tank due to automation. The evacuation of the contents of the tank can be carried out in one or more compressed gas flush, preferably in a single flush of compressed gas.
The first flush can be operated at the latest 60s after the introduction of the powdery substance in the tank, better no later than 30 s after it, and the last flush can be operated, if necessary, no later than 30 min. after the introduction of the powdery substance into the tank, better no later than 15 minutes after it.
When the evacuation of the contents of the tank takes place in a single flush of compressed gas, it is preferably carried out at the latest 60s after the introduction of the powdery substance into the tank, better no later than 30 s after it. The injection of the powder substance into the tank can be carried out through a branching of internal diameter less than or equal to 17 mm, for example between 3 and 17 mm, better between 5 and 15 mm. Such a diameter makes it possible to limit the dead volume and to reduce the risk of fouling.
The mixture may be agitated according to at least two different stirring regimes.
In particular, the mixture may be subjected to stirring at a lower rate (typically by a factor of 0.05 to 0.9, or even zero) at the time of the at least partial emptying, compared to the sequence from the end of the introduction of the powdery substance at the beginning of the emptying. This reduces the risk of formation of gaseous pockets in the exhaust pipe. This also reduces the flow stress at the quilting of the drain.
According to one embodiment, the stirring regime in the tank may be identical from the introduction of the powder substance into the tank until the beginning of the emptying.
According to another embodiment, the mixture may be subjected to stirring in at least two different stirring regimes that are not detrimental from the introduction of the pulverulent substance into the tank until the beginning of the emptying, of which a regime stronger (typically by a factor of 1.1 to 4) between the end of the introduction of the powdery substance and the beginning of the emptying, than at the time of the introduction of the powdery substance into the tank. This reduces the risk of spraying pulverulent substance above the liquid in the tank during the step of introducing it. By way of illustration, the mixture may be subjected to agitation ranging from 400 to 1000 rpm between the end of the introduction of the powdery substance and the beginning of the emptying.
The aqueous medium may contain at least one phytosanitary active agent, the latter being injected into a water pipe connected to the tank. The aqueous medium may in particular contain several phytosanitary active ingredients injected separately by respective taps into said pipe. Such a separate injection facilitates traceability and maintenance. It also significantly reduces clutter in the immediate vicinity of the tank.
This pipe may comprise a direct line opening directly into the tank and a bypass opening therein via at least one washing head, and at least one valve for selectively sending the optionally loaded water of at least a phytosanitary asset in the tank, either via the direct line or via the bypass.
In particular, the water can be sent to the tank by the direct line when it is loaded with the phytosanitary active agent (s). This avoids over-measuring the washing head with the active (s) phytosanitary (s), which reduces the risk of corrosion and also prevents sedimentation eventual phytosanitary (s) lead (s) lead a gradual fouling of the washing head. .
Preferably, a certain quantity of water is sent into the tank once it has been drained, this water circulating through the bypass and the washing head, and being used both for rinsing the tank and in the constitution of the tank. aqueous medium of the next preparation cycle. This limits the amount of waste and the cost of treating the effluents generated by the installation, since the rinsing water can be reused as is from the next preparation cycle. Experience has shown that even by proceeding in this way, the variability in the formulation of the mixture remains within acceptable limits since the constitution of this rinsing water is almost constant from one cycle to another.
The minimum level of depression in the tank just before the aspiration of the powdery substance can be between -0.05 and -1 bar, especially between -0.1 and -0.8 bar, better between -0.3 and -0.3. -0.5 bar. This minimum level of depression is preferably maintained in the tank for the duration of the injection of the powdery substance.
The level of overpressure in the tank during the at least partial emptying operation can be between 0.05 and 2 bar, in particular between 0.1 bar and 1 bar.
The method according to the invention may comprise the atmospheric pressure setting of the tank with a vent during the injection of water, possibly loaded with active (s) in the tank.
The contents of the tank can be immediately emptied automatically to a dedicated container in case of emergency stop, this emergency emptying being triggered by manual pressing a corresponding button.
The process according to the invention is advantageously carried out using at least two tanks in cycles that are out of phase with each other, these tanks being preferably connected to the same source of water and active ingredient (s) and to the same source of powdery substance. The invention also relates to an installation for preparing a seed treatment composition, in particular for implementing the method according to the invention as defined above, comprising at least one tank comprising: at least one stitch located below the level of the aqueous medium in the tank, and connected to an arrival of powdery substance, o one or more connections connected to a water supply line of the tank, this pipe itself having one or more connections allowing an injection therein, a vent, a source of vacuum, a source of compressed air, and o a discharge outlet of the tank to a treatment device where the mixture is brought into contact with the seeds. treat.
The same quilting can be connected to several different departures / arrivals. In a variant, as many taps are used as different arrivals / departures. The plant according to the invention allows the introduction of the powder substance under the level of the aqueous medium in the tank, through a quilting and a depression created in the tank by the vacuum source.
This mode of introduction of the powdery substance is advantageous compared for example to a mode of introduction by a dip tube, especially in the case where the powder substance is a hydratable compound. This limits the risk of fouling of the means for introducing the powdery substance. The plant according to the invention may comprise a washing head in the tank, connected to the water supply pipe of the tank via a bypass. The plant according to the invention may comprise a tank having a capacity of less than or equal to 50 l, better still 20 l, more preferably 10 l, and a capacity greater than or equal to 0.1 l, better still 0.5 l. The size of the tank can be set according to the quantity of seeds to be treated per cycle and the possible number of successive flushes of a compressed gas fixed to completely empty it.
Preferably the installation of the invention comprises conical vessels. The flow of the mixture is thus promoted during the emptying step, which makes it possible to limit the risks of depositing the dispersion containing the powdery substance, especially at the end of the cycle, in particular in the case where the latter is a compound hydratable. The plant according to the invention may comprise an automatic control unit for solenoid valves, motors and / or pumps for cyclically controlling the filling, including the dosing, of the tank in liquid, the dosing then the injection of the powdery substance in the tank, emptying the tank, and stirring therein. The plant according to the invention may comprise two tanks for producing the mixture, adapted to be used in a phase-shifted manner, so that a mixture can be prepared in one of the tanks while a mixture ready for use. job is evacuated from another tank. The plant according to the invention can still be used without addition of powder substance in the tank, to perform seed treatment with one or more active ingredients. Thus, in this case, the arrival nozzle of pulverulent substance is not used, and the corresponding solenoid valve remains closed.
The term "seed" should not be understood with a limiting meaning.
Thus, by "seed (s)" is meant any organ or fragment of a plant that is placed in a culture medium (usually soil) to allow the formation of another plant of the same nature. It can especially be a seed. A seed may be formed of such an organ or plant fragment agglomerated with other substances or with several organs or fragments agglomerated with each other. In addition, the seed to which the treatment process is applied may have previously undergone further treatment. In particular, this seed may have already been treated and, for example, be covered with one or more layers of a coating. Conversely, this seed can be in the natural state. The term "aqueous medium" denotes a medium comprising as a solvent for water, and "dispersion", a heterogeneous system in which a finely divided material, here the powdery material, is distributed in another material, here the aqueous medium.
By "hydratable compound" is meant a compound, for example a polymer, which, when it is dispersed in distilled water at 25 ° C., with stirring for 2 hours, at a concentration of up to 5 hours. % by weight, based on the total weight of the dispersion, led in less than 48 hours under slight stirring, by hydration, to a formulation having a viscosity (measured by a Rheomat RM300 at 25 ° C., at a shear rate of 10 seconds). 1) greater than 8000 cP. In this sense, it is considered that formulations for which no viscosity measurement is possible (for example, totally gelled formulations) have a viscosity (measured by a Rheomat RM300 at 25 ° C, at a shear rate 10s'1) greater than 8000 cP.
For this measurement, the pH value of the dispersion can be adjusted to improve hydration conditions of the hydratable compound. The value of the pH can thus vary typically from 3 to 12, in particular from 5 to 10, depending on the hydratable compound in question, the pH ranges appropriate for each type of hydratable compound being known to those skilled in the art.
The hydratable compound may be present in the mixture used to treat the seeds at a maximum concentration of 70% by weight, based on the weight of the mixture. Advantageously, this concentration is between 4.5 and 70% by weight, for example between 5 and 65% by weight, better between 7.5 and 65% by weight, especially between 10 and 60% by weight.
According to one embodiment, the mixture is brought into contact with the seeds before the viscosity of the mixture (measured at 25 ° C. at a shear rate of 10 seconds by a Rheomat RM300) reaches a maximum value. This maximum value may be greater than or equal to 10,000 cP (centipoise), ie 10000 mPa-s. (milli pascal-seconds), in particular greater than or equal to 50000 cP, ie 50000 mPa-s. The contacting step can thus be carried out before the viscosity of the mixture (measured at 25 ° C. at a shear rate of 10s -1 by a Rheomat RM300) reaches a maximum value of 50000 mPa-s. By way of illustration, the hydratable compound may be chosen in particular from the following compounds: a cellulose or a derivative thereof, for example hydroxycellulose, alkylcellulose, such as methylcellulose, hydroxyalkylcellulose such as hydroxyethylcellulose, or hydroxypropylcellulose, hydroxypropylmethylcellulose, carboxyalkylcellulose, such as carboxymethylhydroxyethylcellulose, sodium carboxymethylcellulose, synthetic polymers such as polyvinylpyridine, polyvinylpyrrolidone, polyethylene glycol, polyethylene oxide, polyamide, polyacrylamide, polymethacrylic acid, polyvinyl alcohol, polyglycerol, polytetrahydrofuran, polyacrylic acid, polyacrylate, alginic acid and its derivatives, such as alginate, pectin, galactomannans and their derivatives, such as guar gum, hydroxypropyl guar gum, carboxymethyl-guar, carboxymethylhydroxypropyl-guar, cationic guars, gelatin, starch and its derivatives, t cationic starch, maize starch, wheat starch, rice starch, potato starch, tapioca, waxy maize, sorghum, waxy sorghum, dextrin, chitin, chitosan, xanthan gum, carrageenan gum, karaya gum, a derivative of any of the aforementioned compounds, or a combination thereof.
According to one embodiment, the hydratable compound is chosen from celluloses and their derivatives.
According to another embodiment, the hydratable compound is chosen from galactomannans and their derivatives.
According to another embodiment, the hydratable compound is chosen from polyacrylamides and their derivatives.
According to another embodiment, the hydratable compound is chosen from starch and its derivatives.
According to another embodiment, the hydratable compound is chosen from xanthan gum and its derivatives.
The hydratable compound is, for example, an agropolymer of natural origin sold under the trademark AgRHO WR 30 or AgRHO GSB 30 by the company Solvay.
It should be noted that the mixture may advantageously comprise other compounds than the hydratable compound, for example, pesticides, fungicides, herbicides, molluscides, bactericides, bacteriostats, repellents, nutrients, fertilizers. growth stabilizers, latexes (for example chosen from polymers of the vinyl acetate, polyurethane, styrene butadiene or acrylic type, optionally in the form of core / shell structures), surfactants, antioxidants, plasticizers, dyes, fillers (for example a fluence powder (or drying powder) of the silica type (in particular precipitated or pyrogenic silicas), kaolin or talc), biological additives (for example inoculants of the bacteria type). or fungi (especially mycorrhizal)) or a mixture thereof. These additional compounds may be added in amounts conventionally used by those skilled in the art. By way of example, the latices may typically be introduced in contents ranging from 2 to 60 g (in dry extract), in particular from 3 to 30 g (in dry extract) per quintal of seed to be treated. The invention makes it possible to obtain a good distribution of the dispersion produced during the mixing operation, on the seeds. This process can be used for the coating of seeds and, in particular, the coating of seeds.
When the dispersion covers a seed, it has a positive influence on the development of this seed. It appears that the dispersal allows the seed to be kept in a moist environment favorable to the development of the seed. This positive influence is, however, noted only if the concentration of hydratable compound in the dispersion is quite high and, in particular, exceeds the minimum concentration mentioned above.
A significant concentration of hydratable compound, however, has the disadvantage of increasing the viscosity of the dispersion. In practice, after adding the hydratable compound in the aqueous medium, the viscosity of the dispersion increases very rapidly. Contacting the hydratable compound and the seeds before the viscosity of the dispersion reaches the above-mentioned maximum value and / or within a certain period of time makes it possible to limit or even avoid the formation of aggregates. . Such aggregates are undesirable because the amount of agglutinated dispersion aggregate is useless in seed treatment and is a waste. Conversely, if there is little or no aggregates, a more homogeneous treatment is obtained: the dispersion is better distributed on the seeds and each seed is better covered by the dispersion. By limiting or avoiding the formation of aggregates in the invention, the risk of fouling of the bowl and the mixing bowl of the seed treatment device, for example the wrapper, in which the dispersion is mixed, is reduced. to seeds.
According to one embodiment, the mass of mixture placed in contact with the seeds may be between 0.5 and 10% of the seed mass.
In some embodiments, the mass of mixture contacted with the seeds is greater than or equal to 0.5% of the seed mass. Below this minimum value of 0.5%, the amount of mixing per seed and, therefore, the effect of mixing on the seeds may not be sufficient. Typically, the seed mass contacted with the seeds may be greater than or equal to 0.75% of the seed mass, in particular greater than or equal to 1% of the seed mass.
Moreover, the mass of mixture placed in contact with the seeds is typically less than or equal to 10% of the seed mass, in particular less than or equal to 8%, in particular less than or equal to 6%. Beyond this maximum value, a saturation effect can be observed. In other words, the excess mixture mass has little or no effect and is a waste. Also, beyond a ratio of 10% between the mass of the mixture and the seed mass, especially above 8%, in particular above 6%, there is a risk that the quantity of water in the mixture exceeds the threshold acceptable by the seed. Beyond this acceptable threshold, the seed can sprout spontaneously or rapidly lose its germinative capacity after some storage time.
Advantageously, the implementation of the treatment method of the invention does not cause excessive hydration of the seeds. In addition, the implementation of the treatment method of the invention does not modify the germination capacity of the seeds.
The minimum and maximum mass ratios between the mass of the mixture and the seed mass may vary between the aforementioned ranges depending on the nature of the seed and the formulation of the mixture, and in particular the nature of the mixture. hydratable compound.
In addition to the features just mentioned, the proposed method may have one or more of the following features, considered individually or in technically possible combinations:
When placed in contact with the seeds, the hydratable compound must already be at least partially hydrated. This partial hydration improves its ability to adhere to the seed. Advantageously, the method of the invention does not require the introduction of additional adhesive solutions to ensure the adhesion of the hydratable compound on the seed.
As indicated above, the concentration of the hydratable compound is preferably between 4.5 and 70% by weight, in particular between 5 and 65% by weight, relative to the weight of the mixture. This concentration may especially be between 10 and 45% by weight, in particular between 15 and 35% by weight. These concentration ranges make it possible to obtain a good compromise, for most hydratable compounds, between the kinetics of rise in viscosity observed and the amount of compound and water in the dispersion.
Optionally, a drying step may be carried out after the seeds are brought into contact with the mixture in order to reduce the amount of water supplied by the mixture. This drying can be done for example by heating at a moderate temperature, for example from 20 to 40 ° C, for a few minutes to a few hours, so that the moisture gain of the seeds resulting from the process of the invention does not exceed About 3% by weight, preferably about 2% by weight.
Advantageously, the method of the invention does not however comprise an additional drying step.
The seeds can be treated in batches or "batches" ranging from 1 to 500 kg, in particular from 10 to 350 kg, in particular from 20 to 300 kg, and a treatment cycle of a batch in the seed treatment device can last less than 1 min. In addition, the proposed method can be integrated into a seed treatment line. In other words, this method can be implemented on seeds previously or after one or more other stages of treatment of these seeds. The invention also relates to treated seeds, in particular coated seeds, obtained according to the method described above.
A non-limiting example of implementation of the invention will now be described, with reference to the accompanying drawing, in which Figures 1 to 4 show a processing plant according to the invention, and Figure 5 a detail of embodiment of a variant of feed quill powder substance.
DETAILED DESCRIPTION
The method according to the invention can be implemented using an installation as shown schematically in FIGS. 1 to 4.
This installation comprises at least one preparation tank 10, and better, as illustrated in FIGS. 1 and 2, two tanks 10 and 10 '.
Each tank 10 or 10 'preferably has a capacity less than or equal to 50 1, better still 20 1, even better at 10 1, and a capacity greater than or equal to 0.1 1, better still 0.5 1, even better at 11.
Each tank 10 or 10 'has various taps 11 to 14 in the upper part, and a tap 15 on its side wall.
In the example considered, each tank 10 and 10 'is for example made of stainless steel which may comprise for example a Teflon-type inner lining and comprises a cylindrical body 16 closed in the lower part by a bottom wall 17, conical and partly upper by a cover 19.
An agitating device 23 is associated with each tank 10 and 10 ', this device comprising a shaft 22 driven in rotation on itself by a motor 20. One or more mixing members 21, identical or different, are mounted on the shaft 22 so as to be rotated by it.
The mixing member (s) 21 may in particular be chosen from Intermig type deflocculators or stirrers.
Stitching 12 feeds at least one 60-360 ° rinsing water spray nozzle into the tank. In the example under consideration, the quilting 12 feeds a rotary spraying ball 24.
The stitching 12 is connected via a solenoid valve 50 to a pipe 25 fed by a water network 27, for example a tap water network, shown in FIG. 4.
As can be seen in this FIG. 4, the pipes 25 connected to the taps 12 of the two tanks 10 and 10 'meet downstream of a section 40 supporting various branchings 30 to 34 of active supply, these connections being arranged, for example, close together according to a montage called "clarinet".
Returning to FIGS. 1 and 2, it can be seen that the tap 13 of each tank 10 or 10 'is connected, via a bypass 42 comprising a solenoid valve 51, to the corresponding pipe 25, upstream of the solenoid valve 50 and downstream of section 40.
Each stitch 14 is connected firstly via a solenoid valve 54 to a vent 55, and secondly to a source of compressed air 57, via a not shown solenoid valve.
The taps 11 of the tanks 10 and 10 'are connected, each via a solenoid valve 58, to a vacuum source 59.
The connections 30 to 34 of the section 40 are connected via respective solenoid valves 60 to 64 to sources of active agents that may be present in the final mixture.
The taps 30 to 34 can be fed by metering pumps through respective flow meters 70 to 74 to know precisely the amount of distributed asset.
The section 40 may be selectively powered by a compressed air network 82 or by the tap water network 27, via solenoid valves 80 and 81 respectively.
Each tapping 15 opens into the corresponding tank 10 or 10 ', below the nominal level of the liquid in the tank during the mixing operation. The tapping 15 opens for example, as illustrated, substantially at the junction between the cylindrical body 16 of the tank and its bottom wall 17.
The stitching 15 may be, as illustrated in Figures 1 and 2, oriented substantially horizontally or, as shown in Figure 5, with a non-zero angle with the horizontal. The stitching 15 is for example oriented obliquely downwards, particularly at 45 ° with respect to the axis of the tank. In this case, it will preferably lead to the cylindrical body 16. The stitching 15 can still be oriented obliquely upwards. In this case, it will lead preferably to the bottom wall 17.
The stitching is preferably of less than or equal to 17 mm inner diameter, for example between 3 and 17 mm, better between 5 and 15 mm.
Each stitching 15 is connected via a solenoid valve 95 to a line 100 for introducing the powdery substance into the tank 10 or 10 '. This pipe 100 is connected, as shown in FIG. 3, to a powder metering system 122 including a hopper 120 supplying a powder transfer system 105 of the worm type (for example twin-screw) or vibrating plate, the whole it can be mounted on a scale 121 in order to know by difference the quantity delivered.
The pipe 100 is advantageously formed over at least part of its length by a flexible pipe 106, preferably at least partially transparent. This facilitates maintenance in case of clogging of the pipe 100. The solenoid valve 95 preferably comprises a full-bore ball-type valve, whose outlet pipe can be fixed at a small distance on the wall of the tank so as to limit the dead volume. The evacuation of the contents of each tank 10 or 10 'is done through a drain hole 126 at the low point of the bottom wall 17, this opening opening via a solenoid valve 130 on a pipe The solenoid valve 130 is preferably equipped with a ball type valve.
Line 135 is connected to a three-way solenoid valve 140, which makes it possible to selectively connect line 135 either to a waste collection container 145 or to a supply line 150 for a treatment device such as a wrapper. not shown in the drawing. Preferably, as illustrated, the connection of the solenoid valve 140 to the container 145 and the treatment device is via flexible hoses 147 and 148, preferably stainless PTFE braided, which facilitates the evacuation of the dispersion. The three-way solenoid valve 140 is preferably equipped with a ball type valve.
A non-intrusive flowmeter 160 may be disposed downstream of the three-way solenoid valve 140 to control it in order to interrupt the emptying of the corresponding tank 10 or 10 'at the end of each supply cycle of the treatment device. one of the vats.
Compressed air can be injected into the section between the solenoid valves 130 and 140 via a solenoid valve 170, connected to the compressed air network, to purge the pipes at the end of use. The shaft 22 of the stirring device may be centered or off-center with respect to the axis of the vessel.
The operation of the installation is as follows. The various solenoid valves, pumps and motors are controlled by an automaton. The latter controller receives information from the various sensors of the installation, including pressure, flow and weight.
Vats 10 and 10 'are preferably used in parallel, out of phase with masked time preparation of the mixture in one of the tanks while the mixture contained in the other tank is sent to the treatment device, and vice versa. In the following, the method is described for the tank 10 only, being the same for the tank 10 'in a time-shifted manner.
The tank 10 is first supplied with water and active ingredients by the tap 13 and then with water through the tap 12, until the level of liquid in the tank corresponds to a predefined quantity depending on the final concentration to be obtained. in pulverulent material in the mixture. This level of liquid is sufficient for the stitching 15 to be immersed. The volume of the mixture is preferably less than or equal to 151, more preferably 101. During filling, the solenoid valve 54 is open, to open the communication to the vent 55. The water supply via the washing head 24 allows to clean the emergent part of the tank of the possible deposits left by the preceding cycle of preparation.
Then, the solenoid valves 50, 51 and 54 being closed, the solenoid valve 58 is opened, to put the tank in depression via the nozzle 11. Once the sufficient vacuum level is reached, the solenoid valve 95 is opened to allow the injection at least one pulverulent substance previously weighed and stored in the powder feed tank 123 below the liquid level. The minimum level of depression in the tank just before the aspiration of the powdery substance is preferably between -0.05 and -1 bar, especially between -0.1 and -0.8 bar, better between -0.3. and -0.5 bar. Such a level of depression allows a satisfactory suction of the powder substance while preventing it from being sucked too violently and through the liquid to the lid, which would cause fouling of the emerged walls and the emission of dust. During injection of powdery substance, the depression is maintained at a sufficient value. The mixture is then subjected to stirring in a first regime.
Then, the solenoid valves 58 and 95 are closed, and the mixture is subjected to a second stirring regime. This second regime is stronger, typically by a factor of 1.1 to 4, than the first. This second regime can extend until the beginning of the emptying of the tank 10.
Once the mixture is ready to be sent to the seed treatment device, which is for example a coater of the compressed air is sent by the tapping 14 and the solenoid valve 130 is open.
Once the planned quantity has been delivered, the solenoid valve 130 is closed.
The mixture may be subjected during the evacuation of the tank 10 to stirring at a third lower rate, typically a factor of 0.05 to 0.9 (or zero), than the second.
The total emptying of the contents of the tank can be achieved either with a single flush of a compressed gas, or with several consecutive flushes of a compressed gas. The evacuation of the contents of the tank can thus be done in a discontinuous manner, to avoid an excessive flow of mixture in the treatment device. In this case, the solenoid valve 130 is open at intervals.
The first flush may be carried out at the latest 60s after the introduction of the powdery substance into the tank, better no later than 30 s after it, and the last flush may be carried out, if necessary, not later than 30 min after introduction of the powdery substance into the vat, preferably at the latest 15 minutes after it.
The level of overpressure in the tank 10 during the at least partial emptying operation is preferably between 0.05 and 2 bar, in particular between 0.1 bar and 1 bar.
When the emptying of the tank is fractionated, that is to say when it is carried out via several consecutive hunts of a compressed gas, the volumes drained during each flush can be identical or different. These volumes are determined according to the quantity of seeds to be treated.
The flow meter 160 makes it possible to know the quantity of mixture sent to the processing device, and informs the automaton.
Once the tank 10 is substantially drained, the next preparation cycle can be started, while the mixture prepared in the tank 10 'can be sent to the seed treatment device.
Of course, the invention is not limited to the example just described. The installation may have only one preparation tank, or alternatively more than two tanks. The plant can also be used, if necessary, to prepare a mixture without pulverulent substance, by introducing one or more assets through the connections 30 to 34, and by mixing them with water sent into the tank 10 or 10. .
Several powder metering systems can be used to feed the tank with different powdery substances. Thus, the mixture may comprise different powdery substances.

权利要求:
Claims (13)
[1" id="c-fr-0001]
1. Seed treatment method, using a composition obtained extemporaneously by mixing at least one pulverulent substance and an aqueous medium, comprising the steps of: - performing automatically and cyclically the mixture in at least a first tank (10; 10 ') by first introducing at least a portion of the aqueous medium and then the powder substance, the latter being sucked into the aqueous medium in the tank through a depression created in the tank at least partially emptying, by means of at least one flushing of a compressed gas into the tank, its contents to a seed treatment device where the mixture is brought into contact with the seeds.
[2" id="c-fr-0002]
2. Method according to claim 1, the pulverulent substance being a hydratable compound.
[3" id="c-fr-0003]
3. Method according to one of the preceding claims, the volume of the mixture in the tank being less than or equal to 151, better 101.
[4" id="c-fr-0004]
4. Method according to any one of the preceding claims, the first flush being operated at the latest 60s after the introduction of the powdery substance in the tank, better at the latest 30 s after it and the last flush being operated on. if necessary at the latest 30 min after the introduction of the powdery substance into the tank, better at the latest 15 min after this one.
[5" id="c-fr-0005]
5. Method according to any one of the preceding claims, the injection of the powder substance into the tank being effected through a stitching with an internal diameter less than or equal to 17 mm, for example between 3 and 17 mm, better understood. between 5 and 15 mm.
[6" id="c-fr-0006]
6. Method according to the preceding claim, the mixture being subjected to stirring at a lower rate, typically by a factor of 0.05 to 0.9, or even zero, at the time of the at least partial emptying, compared to the sequence ranging from end of the introduction of the powdery substance at the beginning of the emptying.
[7" id="c-fr-0007]
7. Method according to any one of the preceding claims, the minimum level of depression in the tank just before the suction of the powdery substance being between -0.05 and -1 bar, in particular between -0.1 and -0 , 8 bar, better between -0.3 and -0.5 bar.
[8" id="c-fr-0008]
8. Method according to the preceding claim, the minimum level of depression being maintained in the tank for the duration of the injection of the powder substance.
[9" id="c-fr-0009]
9. Method according to any one of the preceding claims, the level of overpressure in the tank during the at least partial emptying operation being between 0.05 and 2 bar, in particular between 0.1 bar and 1 bar.
[10" id="c-fr-0010]
Plant for the preparation of a seed treatment composition, in particular for carrying out the process according to any one of the preceding claims, comprising at least one tank comprising: at least one tapping situated below the level of the aqueous medium; in the tank, and connected to an arrival of powdery substance, o one or more connections connected to - a water supply line of the tank, this pipe itself having one or more connections allowing an injection therein active (s), - a vent (55), - a vacuum source (59), - a source of compressed air (57), and o a drain outlet (126) from the tank to a treatment device where the mixture is brought into contact with the seeds to be treated.
[11" id="c-fr-0011]
11. Installation according to claim 10, comprising a washing head (24) in the tank, connected to the water supply pipe of the tank via a bypass.
[12" id="c-fr-0012]
12. Installation according to one of claims 10 or 11, the vessel having a capacity less than or equal to 50 1, better to 20 1, even better to 10 1, and a capacity greater than or equal to 0.1 1, better to 0.5 1, even better at 11.
[13" id="c-fr-0013]
13. Installation according to any one of claims 10 to 12, comprising a controller for controlling solenoid valves, motors and / or pumps for cyclically controlling the filling, including the dosage, the tank liquid, the dosing then the injection of the powder substance into the tank, emptying the tank and stirring therein.

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同族专利:

公开号 | 公开日

WO2017089342A1|2017-06-01|

CN108602033A|2018-09-28|

BR112018010549A2|2018-11-13|

AU2016358613A1|2018-06-28|

US11266059B2|2022-03-08|

FR3043882B1|2017-12-15|

CA3006264A1|2017-06-01|

EP3380221A1|2018-10-03|

US20180352720A1|2018-12-13|

引用文献:

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JP3095118B2|1995-11-29|2000-10-03|矢崎総業株式会社|Seed supply tank for gel coating equipment|

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CN104607091B|2014-12-04|2016-10-05|佛山市特赛化工设备有限公司|A kind of discharging not airborne dust vacuum enters powder method|US11252855B2|2017-08-23|2022-02-22|KSi Conveyor, Inc.|Agricultural seed treatment control system for liquid agrochemicals|

RU2715689C1|2019-05-28|2020-03-02|Федеральное государственное бюджетное научное учреждение "Всероссийский научно-исследовательский институт защиты растений" |Grain treatment process control system|

CN111001350B|2020-01-07|2021-12-21|长沙理工大学|Full-automatic rock-like sample stirring machine capable of preventing dust from being stirred uniformly and stirring method|

CN113079743B|2021-05-19|2021-11-16|黑龙江省农业机械工程科学研究院|Seed nutrition enrichment strengthening machine and enrichment strengthening method based on water permeation alternating vacuum technology|

法律状态:
2016-10-14| PLFP| Fee payment|Year of fee payment: 2 |

2017-05-26| PLSC| Publication of the preliminary search report|Effective date: 20170526 |

2017-10-12| PLFP| Fee payment|Year of fee payment: 3 |

2018-10-11| PLFP| Fee payment|Year of fee payment: 4 |

2019-10-15| PLFP| Fee payment|Year of fee payment: 5 |

2020-10-13| PLFP| Fee payment|Year of fee payment: 6 |

2021-11-09| PLFP| Fee payment|Year of fee payment: 7 |

优先权:

申请号 | 申请日 | 专利标题

FR1561306A|FR3043882B1|2015-11-24|2015-11-24|PROCESS FOR TREATING SEEDS|FR1561306A| FR3043882B1|2015-11-24|2015-11-24|PROCESS FOR TREATING SEEDS|

PCT/EP2016/078420| WO2017089342A1|2015-11-24|2016-11-22|Seed treatment method|

EP16805030.0A| EP3380221A1|2015-11-24|2016-11-22|Seed treatment method|

BR112018010549A| BR112018010549A2|2015-11-24|2016-11-22|seed treatment method|

CN201680079897.9A| CN108602033A|2015-11-24|2016-11-22|Method for treating seeds|

AU2016358613A| AU2016358613A1|2015-11-24|2016-11-22|Seed treatment method|

CA3006264A| CA3006264A1|2015-11-24|2016-11-22|Seed treatment method|

US15/778,733| US11266059B2|2015-11-24|2016-11-22|Seed treatment method|

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